LPhD099 Soil Mineral Determination

Details
Responsible DepartmentDepartment of Basic Science and Environment

Course DatesThree weeks either full-time or part-time during one semester. Individualy decided.
 
Course AbstractThe Ph.D. provides the student with the practical training and theoretical background for performing and interpreting soil mineral identifications, characterizations and determinations by modern instrumental techniques, in particular powder X-ray diffractionand infrared analysis.
 
Course RegistrationFurther information, Email: haha@life.ku.dk
 
Deadline for RegistrationIndividual registration
 
Credits6 (ECTS)
 
Level of CoursePhD course
 
Organisation of TeachingThree weeks either full-time or part-time during one semester
 
Language of InstructionEnglish
 
Course Content
The main areas covered by the course include:
Basic principles of the composition and structure of soil minerals.
Powder X-ray diffraction analysis of soil clay, silt and sand fraction and pure minerals. Training in preparation of unoriented and oriented specimens, in running the X-ray diffractometer (transmission and reflection modes), and in interpretation of the X-ray diffractograms.
Fourier Transform Infrared Analysis (FT-IR) of soil clays and pure minerals. Training in specimen preparation, in running the spectrometer (transmission, diffuse reflectance and attenuated total reflectance modes), and in interpretation of the spectra.
Quantification of the composition of soil clay fractions by integration of results obtained from X-ray diffraction, FT-IR , element analysis, thermal analysis and cation exchange capacity.
Spectroscopic techniques such as Mössbauer spectroscopy, nuclear magnetic resonance (NMR), electron spin resonance(ESR) and microscope techniques such as scanning electron microscopy, scanning tunneling microscopy, atomic force microscopy and lighte microscopyof thin sections are briefly considered.
 
Teaching and learning Methods
Three weeks either full-time or part-time during one semester
 
Learning Outcome
The Ph.D. provides the student with the practical training and theoretical background for performing and interpreting soil mineral identifications, characterizations and determinations by modern instrumental techniques, in particular powder X-ray diffractionand infrared analysis.
 
Course Material
Wilson, M.J. (1987,1994) A Handbook of Determinative methods in clay mineralogy. Blackieand Chapman & Hall, London.
 
Course Coordinator
Hans Chr. Bruun Hansen, haha@life.ku.dk, Department of Basic Sciences and Environment/Soil and Environmental Chemistry, Phone: 353-32418
 
Other Lecturers
Christian Bender Koch
 
Course Fee
Free of charge for Ph.D. students under the Open Market for Postgraduate Courses inDenmark and from NOVA-partners.
 
Course Costs
None
 
Type of Evaluation
Written report on experimental work
 
Other Remarks
Special prerequisites: B.Sc. course in Pedology or equivalent